Hostname: page-component-586b7cd67f-t7fkt Total loading time: 0 Render date: 2024-11-23T15:26:44.328Z Has data issue: false hasContentIssue false

Nonlinear Equations for High Accuracy X-Ray Crystal Orientation

Published online by Cambridge University Press:  06 March 2019

Danut Dragoi*
Affiliation:
Enterprise for Research and Production of Semiconductor Materials Sos. Garii Catelu Str., 5 Sector 3, Bucharest, Romania
Get access

Abstract

Nonlinear equations are given for determining the crystallographic orientation of surfaces of single crystals. The equations are solved by an iterative method in several variables. The angle ϕ between the surface plane and the lattice plane in question is decomposed into two components α and β. These two components are obtained from the solution of a non-linear system of equations using two measurements and the Bragg angle. The diffractometric system considered is the well known θ/2θ with a sufficiently large area of x-ray detection and the capability of holding single crystal samples. The results obtained are discussed from experimental and theoretical points of view.

Type
IX. XRD Applications: Detection Levitts, Superconductors, Organics, Minerals
Copyright
Copyright © International Centre for Diffraction Data 1991

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

ASTM F26-84. (1984). “Standard Method for Determining the Orientation of a Semiconductive Single Crystal”, American Society for Testing and Materials. 1916 Race Str. Philadelphia PA.Google Scholar
ASTM E82-84. (1984).“Standard Method for Determining the Orientation of a Metal Crystal”, ibid.Google Scholar
ASTM F 847-83 (1983). “Measuring Crystallographic Orientation of Flats on Single Crystal Silicone Slices and Wafers by X-Ray Techniques”, ibid.Google Scholar
ASTM F 848-83 (1983). “Standard Method for Determining the Lattice Constant of Single Crystal Gadolinium Gallium Garnet”, ibid.Google Scholar
Dragoi, D. (1993) J. Appl. Cryst.. in the press.Google Scholar
Kantorovich, L.V. & Akilov, G.P. (1977). Functionalinii Analiz, Moskva, Nauka.Google Scholar
Lal, K., Bhagavannarayana, G., Kumar, V., Halder, S.K. (1990). Meas. Sci. Technol. 1, 793800.Google Scholar