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An Automated X-Ray Diffractometer for Detection and Identification of Minor Phases

Published online by Cambridge University Press:  06 March 2019

John C. Russ
Affiliation:
School of Engineering, North Carolina State University, P.O. Box 5995, Raleigh, NC 27650
Thomas M. Hare
Affiliation:
School of Engineering, North Carolina State University, P.O. Box 5995, Raleigh, NC 27650
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Extract

In the preceding volume in this series, we described a stepping motor automation package for XRD data acquisition, based on the Apple microcomputer with an interface card that produces the stepping motor pulses and counts X-ray pulses from the normal X-ray detector and amplifier. We are presently using the system to automate a General Electric XRD-5 diffractometer mechanism, by replacing the original synchronous motor with the stepping motor, and installing 10:1 reduction gear instead of the chain drive to drive the double worm gears. This gives 2500 steps of the motor per degree two theta. Motor pulses are counted by a small machine language routine which also handles accelerating the mechanism when slewing over long angular ranges.

Type
IV. XRD Applications and Automation
Copyright
Copyright © International Centre for Diffraction Data 1982

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