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15 - Flow Chart and Processing Procedures for Rock Samples

Published online by Cambridge University Press:  04 April 2011

Harald Strauss
Affiliation:
Ruhr-Universität Bochum
David J. Des Marais
Affiliation:
Ames Research Center
J. M. Hayes
Affiliation:
Indiana University
Toby B. Moore
Affiliation:
University of California
J. William Schopf
Affiliation:
University of California
J. William Schopf
Affiliation:
University of California, Los Angeles
Cornelis Klein
Affiliation:
University of New Mexico
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Summary

Investigation of a large number of samples during this project led to development of the following processing routine.

Curation of samples was performed at the University of California, Los Angeles. As appropriate, subsamples were subsequently distributed to PPRG members for analyses to be carried out at their home institutions. A flow chart outlining the various procedures involved is shown in Figure 15.2 and is summarized below.

The initial curation for every incoming rock sample consisted of assigning a PPRG Sample Number (e.g., “1001”). Pertinent geological information was compiled and entered into the databases “Inventory,” “Site,” and “Strat” (see Chapter 21).

For paleontological and mineralogical studies, petrographic thin sections were prepared of each sample: for microfossil studies, a 150µi-thick “paleo”-section (“1001-1-A”); and for petrographic studies, either a standard 30 µm-thick section for non-carbonates (“1001-1-B”) or a 5 to 15 µm-thick section for carbonates (“1001-1-C”). In addition, large-area thin sections (150 µm-thick, “1001-1-STROM”) were prepared of selected stromatolitic samples.

Sample processing for geochemical and/or palynological studies was initiated by discarding any weathered surface or secondarily emplaced vein material and generating a mass of clean interior rock chips ≤ 1 cm in diameter (“1001-1-RC”). Chipping of small samples was performed using a geologic hammer; larger samples were chipped with a jawbone (i.e., “chipmunk”) crusher. In order to remove any organic contaminants, the chips were etched in a 20% HF-10% HC1 solution, then rinsed with large volumes of distilled water and dried in a drying oven at 75° C.

Type
Chapter
Information
The Proterozoic Biosphere
A Multidisciplinary Study
, pp. 695 - 698
Publisher: Cambridge University Press
Print publication year: 1992

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