Opus signinum is a lime mortar mix that includes crushed pottery as an aggregate. Because it is water-resistant, it was used to line hydraulic structures like pools and aqueducts. While there have been numerous recreations of Roman ‘concretes’ in the past, hydrophobic linings have received little attention, and all preliminary studies in these recreations have paid more attention to the dry components and the lime than to the hydric needs of the mortar. The experiment presented here was to gain a better understanding, with the help of traditional builders, of the process of mixing and applying hydrophobic linings and calculate the water consumption of individual samples. The data obtained contribute to assessing the water consumption needs on Roman construction sites, what associated logistics these volumes required, and what the technicalities of applying this specific type of lining were.

Research on prehistoric mainland Southeast Asia is dominated by mortuary contexts, leaving processes such as the transition to sedentism relatively understudied. Recent excavations in southern Vietnam, however, have recovered new evidence for settlement. The authors report on investigations at the neolithic site of Loc Giang (3980–3270 cal BP) in southern Vietnam, where excavation revealed a vertical sequence of more than 30 surfaces. Microarchaeological analyses indicate that these features are carefully prepared lime mortar floors; the lime was probably produced from burnt shell. The floors date to between 3510 and 3150 cal BP, providing the earliest-known evidence for the use of lime mortar, and for durable settlement construction, in this region.

Radiocarbon (14C) dating of anthropogenic carbonates (CaCO3) such as ash, lime plaster and lime mortar, has proven a difficult task due to the occurrence of a number of contaminants embedded within the CaCO3 pyrogenic binder. These include 14C-free geologic components and/or secondary phases bearing an unknown amount of 14C, and thus the alteration of the original pyrogenic isotopic signature of the material results in major age offsets when carbon recovery is performed through acid hydrolysis. Here we present a characterization/quantification approach to anthropogenic carbonates that includes Fourier transform infrared spectroscopy (FTIR), X-ray diffraction, thin section petrography, thermogravimetric analysis and scanning electron microscopy coupled with high-resolution cathodoluminescence, with which we identified the pyrogenic CaCO3 fraction in an aerial lime plaster and two hydraulic mortars. The preserved pyrogenic component was then isolated by density separation and its purity checked again using FTIR. Carbon was recovered through thermal decomposition in vacuum. The resulting 14C age matches the expected age of the lime plaster, whereas hydraulic mortars are slightly offset due to the carbonation of calcium hydroxide lumps. This approach highlights the importance of a dedicated characterization strategy prior to dating and may be applied to aerial lime plasters to obtain accurate ages.