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1 results

  • Crystal structure and diffraction data for a polymorph of voglibose (C10H21NO7)

  • G. Q. Zhang, G. L. Lv
  • Journal:
    Powder Diffraction / Volume 25 / Issue S1 / September 2010
    Published online by Cambridge University Press:
    06 March 2012, pp. S28-S30

  • X-ray powder diffraction data of voglibose are reported, and its crystal and molecular structures were determined by simulated annealing and rigid-body Rietveld refinement methods. Voglibose was found to be crystallized in triclinic symmetry with space group P-1. The lattice parameters were determined to be a=6.1974(6) Å, b=6.9918(5) Å, c=7.3955(9) Å, α=70.8628(3), β=103.5312(4), γ=94.3867(5)°, V=294.2(2) Å3, and ρcal=1.495 g/cm3. The crystal structure contains isolated C10H21NO7 molecular.