Artefacts in quartzite have been found in a unique topographical location on the highest terrace of the Rhône Valley in France. These discoveries offer new opportunities for dating early European occupations.

Several quartzite bodies outcrop along the Ferreira-Ficalho Thrust Fault (South Portugal), a major accident of the Iberian Variscan Orogen. The sediment is a very pure quartz sandstone, with trace amounts of ultra-resistant heavy minerals and chromite. Chemical characterization (microprobe analyses and Mössbauer spectroscopy) showed the chromite to be unique: besides being Zn-rich, complexly zoned and a cation deficient spinel, all the iron was found to be fully oxidized to Fe3+. Structure refinement of single-crystal X-ray diffraction intensities unambiguously identifies the mineral as a chromite and the Mössbauer data are consistent with tetrahedrally coordinated Fe3+ in the spinel structure. Current geodynamical models see the Ferreira-Ficalho Thrust Fault as a first-order suture resulting from a complex collision of two distinct continental blocks with partial obduction of the intervening oceanic crust. The chromite grains could be envisaged as remnants of an early erosion of this obducted oceanic crust, but its unique chemical character does not allow any definite conclusion. Yet, the complete quartzite heavy mineral contents and its petrographic features are not consistent with their deposition within a continental collision situation.

This paper describes a newly observed phenomenon, a rare form of lamina protecting petroglyphs from weathering, and it attempts an explanation of such features. These laminae are not precipitates but represent the floors of the original cupules that have become more resistant to erosion through conversion to tectonite. The process involves crystallization of the syntaxial quartz overgrowths on quartz grains that constitute the cement component of quartzite and silica-rich schist. It is attributed to the cumulative application of kinetic energy that derives from the tens of thousands of hammerstone blows that produced the cupule. The tribological process results in products similar to those formed in ductile shear zones when sandstone has been subjected to great kinetic stresses. In the cupules reported here, the re-metamorphosed lamina preserves their original surface and prevents the erosion of the protolith (parent rock) concealed by the modified layer. The thickness of the layer is a function of the cumulative amount of energy applied to the rock's cement, and the process of alteration is defined as ‘kinetic energy metamorphosis’.

One of the advantages of a multidetector neutron time-of-flight diffractometer such as the high pressure preferred orientation diffractometer (HIPPO) at the Los Alamos Neutron Science Center is the capability to measure efficiently preferred orientation of bulk materials. A routine experimental method for measurements, both at ambient conditions, as well as high or low temperatures, has been established. However, only recently has the complex data analysis been streamlined to make it straightforward for a noninitiated user. Here, we describe the Rietveld texture analysis of HIPPO data with the computer code Materials Analysis Using Diffraction (MAUD) as a step-by-step procedure and illustrate it with a metamorphic quartz rock. Postprocessing of the results is described and neutron diffraction results are compared with electron backscatter diffraction measurements on the same sample.

The susceptibility of rocks to weathering into soils and the subsequent weathering of the solum itself are important both with respect to sediment formation and to agriculture. Residual soils developed on some rock types representative of the major soil associations of NE Scotland have consequently been examined in detail in an attempt to assess the weatherability of both the rocks and the derived soils. Methods based on chemical composition have been supplemented by potential methods related to the production of poorly-ordered aluminosilicate material and to depolymerisation of the silicate framework in the minerals present. In general, there is, as would be expected on the basis of increasing energy supply and increasing entropy, an increase in the amount of monomeric silica towards the surface and this appears to be closely related to the amount and nature of the poorly-ordered aluminosilicate. The results suggest that only the purely chemical methods can currently enable a reasonable assessment to be made of the susceptibility of a rock or soil to further weathering.