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1 results

  • Understanding the Effects of Graphene Coating on the Electrostatic Field at the Tip of an Atom Probe Tomography Specimen

  • Florant Exertier, Jiangting Wang, Jing Fu, Ross K.W. Marceau
  • Journal:
    Microscopy and Microanalysis / Volume 28 / Issue 4 / August 2022
    Published online by Cambridge University Press:
    30 July 2021, pp. 1054-1065
    Print publication:
    August 2022

  • As a three-dimensional characterization method, atom probe tomography can provide key information that other methods cannot offer. Conductive coatings have proved to be an effective way for biological samples, and nonconductive samples in general, to be analyzed using voltage-pulsed atom probe tomography. In this study, we analyzed the effects of graphene coating on an electrically conductive material and were able to confirm the detection of carbon atoms. We compare quantitative electrostatic field metrics for a single-coated and a multi-coated specimen and measure both a reduced voltage after graphene coating and lowered charge-state ratios for different ion species, suggesting a lowered evaporation field related to the graphene coating. This information will be instructive for future studies on graphene-coated, nonconductive biological specimens.