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Processing of Superconducting Ceramics Using Microwave Energy

Published online by Cambridge University Press:  21 February 2011

Iftikhar Ahmad
Affiliation:
Department of Materials Science and Engineering, University of Florida, Gainesville, FL 32611
G. T. Chandler
Affiliation:
Department of Materials Science and Engineering, University of Florida, Gainesville, FL 32611
D. E. Clark
Affiliation:
Department of Materials Science and Engineering, University of Florida, Gainesville, FL 32611
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Abstract

Superconducting ceramics have been successfully prepared employing a novel internal heating mechanism which uses microwave energy. Calcining with microwaves requires further investigation to improve the superconducting properties. Sintering and annealing in microwave energy shows refined microstructure and improved oxygen content in the YBa2Cu3O7-x phase. This is attributed to the coupling of CuO with microwave energy. The onset of the superconductive transition occurs at 93°K for the conventionally calcined/microwave annealed samples. The conventionally processed samples have an onset transition at 90°K and exhibit weaker diamagnetism when compared with the microwave annealed sample.

Type
Research Article
Copyright
Copyright © Materials Research Society 1988

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References

REFERENCES

1. Bednorz, J.G. and Muller, K.A., Z. Phys. B64, 189 (1986).CrossRefGoogle Scholar
2. Jin, S., Tiefel, T.H., Sherwood, R.C., Kammlott, G.W. and Zahurak, S.M. App. Phys. Lett. 51(12) 943 1987.CrossRefGoogle Scholar
3. Johnson, D.W. Jr., Gyorgy, E.M., Rhodes, W.W., Cava, R.J., Feldman, L.C. and van Dover, R.B., Adv. Ceram. Mater. 2, 364 (1987).CrossRefGoogle Scholar
4. Chabinsky, I.J. and IIIEves, E. E., presented at the AGM of the American Ceramic Society, Chicago 1985.Google Scholar
5. Wang, G., Hwu, S.-J., Song, S.N., Ketterson, J.B., Marks, L.D., Poeppelmeier, K.R. and Mason, T.O., Adv. Ceram. Mater. 2, 313 1987.CrossRefGoogle Scholar
6. Frase, K.G. and Clarke, D.R., Adv. Ceram. Mater. 2, 295 (1987).CrossRefGoogle Scholar
7. Brook, R.J., Mat. Sci. and Eng. 71, 305 (1985).CrossRefGoogle Scholar
8. Mostagachi, H. and Brook, R.J., Trans. J. Br. Ceram. Soc. 82, 167 (1983).Google Scholar
9. Walkiewicz, J.W. and McGill, S.L., presented at the 89th Annual Meeting of the American Ceramic Society Inc., Pittsburgh, PA, 1987.Google Scholar
10. Oyanagi, H., Ihara, H., Matsubara, T., Tokumoto, M., Matsushita, T., Hirabayashi, M., Murata, K., Terada, N., Yao, T., Iwaski, H. and Kimura, Y., Japn. J. Appl. Phys., Vol.26, No. 9, L1561 (1987).CrossRefGoogle Scholar
11. Jorgensen, J.D., Beno, M.A., Hinks, D.G., Soderholm, L., Volin, K.J., Hitterman, R.L., Grace, J.D., Schuller, K., Segre, C.U., Zhang, K. and Kleefisch, M.S., Phys. Rev. B, Vol.36, No. 7, 3608 1987.CrossRefGoogle Scholar
12. Dagani, Ron, C & EN, p. 4, March 14, 1988.CrossRefGoogle Scholar