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The Making of LaB6 Crystals

Published online by Cambridge University Press:  14 March 2018

Damon L. Heer*
Affiliation:
FEI Company

Extract

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The following image is of a LaB6 crystal formation created at the FEI Company, Hillsboro, Oregon. The photograph was taken through a Bausch & Lomb Stereo Zoom 4 at 30X with a Polaroid MicraCam.

The single crystal LaB6 and CeB6 is grown and fabricated at FEI using a well-defined process known as "Inert Gas Arc Float Zone Refining." This process takes place in an inert gas atmosphere and utilizes an electrical arc to melt the hot, pressed powder sample of LaB6 or CeB6. This not only allows the growth of the crystal, but also hefps to purify the material. Through research and 20 years of experience in the growth of rare-earth boride single crystals, FEI can carefully control the material composition (e.g. stoichiometry of B/La) tor the highest possible ratio of electron emission to evaporation rate.

Type
Research Article
Copyright
Copyright © Microscopy Society of America 1995