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Spatial and Compositional Biases Introduced by Position Sensitive Detection Systems in APT: A Simulation Approach

Published online by Cambridge University Press:  13 February 2019

C. Bacchi*
Affiliation:
Normandie Université, UNIROUEN, INSA Rouen, CNRS, Groupe de Physique des Matériaux, 76000 Rouen, France
G. Da Costa
Affiliation:
Normandie Université, UNIROUEN, INSA Rouen, CNRS, Groupe de Physique des Matériaux, 76000 Rouen, France
F. Vurpillot
Affiliation:
Normandie Université, UNIROUEN, INSA Rouen, CNRS, Groupe de Physique des Matériaux, 76000 Rouen, France
*
*Author for correspondence: C. Bacchi, E-mail: [email protected]
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Abstract

Due to the low capacity of contemporary position-sensitive detectors in atom probe tomography (APT) to detect multiple events, material analyses that exhibit high numbers of multiple events are the most subject to compositional biases. To solve this limitation, some researchers have developed statistical correction algorithms. However, those algorithms are only efficient when one is confronted with homogeneous materials having nearly the same evaporation field between elements. Therefore, dealing with more complex materials must be accompanied by a better understanding of the signal loss mechanism during APT experiments. By modeling the evaporation mechanism and the whole APT detection system, it may be possible to predict compositional and spatial biases induced by the detection system. This paper introduces a systematic study of the impact of the APT detection system on material analysis through the development of a simulation tool.

Type
Instrumentation and Experimental Methodology
Copyright
Copyright © Microscopy Society of America 2019 

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References

Blavette, D & Sauvage, X (2016). Early developments and basic concepts. In Atom Probe Tomography, Lefebvre-Ulrikson, W, Vurpillot, F and Sauvage, X (Eds.), pp. 115. London, United Kingdom: Academic Press. Available at http://linkinghub.elsevier.com/retrieve/pii/B9780128046470000012 (retrieved July 9, 2018).Google Scholar
Da Costa, G (2016). Atom probe tomography. In Atom Probe Tomography, Lefebvre-Ulrikson, W, Vurpillot, F and Sauvage, X (Eds.), pp. 155181. London, United Kingdom: Academic Press. Available at http://linkinghub.elsevier.com/retrieve/pii/B9780128046470000061 (retrieved July 9, 2018).Google Scholar
Da Costa, G, Vurpillot, F, Bostel, A, Bouet, M & Deconihout, B (2005). Design of a delay-line position-sensitive detector with improved performance. Rev Sci Instrum 76, 013304.Google Scholar
Da Costa, G, Wang, H, Duguay, S, Bostel, A, Blavette, D & Deconihout, B (2012). Advance in multi-hit detection and quantization in atom probe tomography. Rev Sci Instrum 83, 123709.Google Scholar
Danoix, F, Miller, M & Bigot, A (2001). Analysis conditions of an industrial Al–Mg–Si alloy by conventional and 3D atom probes. Ultramicroscopy 89, 177188.Google Scholar
De Geuser, F, Gault, B, Bostel, A & Vurpillot, F (2007). Correlated field evaporation as seen by atom probe tomography. Surf Sci 601, 536543.Google Scholar
Jagutzki, O, Mergel, V, Ullmann-Pfleger, K, Spielberger, L, Meyer, U, Doerner, R & Schmidt-Boecking, HW (1998). Fast position and time-resolved read-out of micro-channel plates with the delay-line technique for single-particle and photon-detection. In International Symposium on Optical Science, Engineering, and Instrumentation Descour, MR & Shen, SS (Eds.), p. 322. Available at http://proceedings.spiedigitallibrary.org/proceeding.aspx?doi=10.1117/12.328113 (retrieved July 11, 2018).Google Scholar
Jagutzki, O, Mergel, V, Ullmann-Pfleger, K, Spielberger, L, Spillmann, U, Dörner, R & Schmidt-Böcking, H (2002). A broad-application microchannel-plate detector system for advanced particle or photon detection tasks: Large area imaging, precise multi-hit timing information and high detection rate. Nucl Instrum Methods Phys Res Sect A 477, 244249.Google Scholar
Meisenkothen, F, Steel, EB, Prosa, TJ, Henry, KT & Prakash Kolli, R (2015). Effects of detector dead-time on quantitative analyses involving boron and multi-hit detection events in atom probe tomography. Ultramicroscopy 159, 101111.Google Scholar
Miller, MK & Forbes, RG (2014). Atom-Probe Tomography. Boston, MA: Springer US. Available at http://link.springer.com/10.1007/978-1-4899-7430-3 (retrieved July 9, 2018).Google Scholar
Miller, MK & Smith, GDW (1981). An atom probe study of the anomalous field evaporation of alloys containing silicon. J Vac Sci Technol 19, 5762.Google Scholar
Peng, Z, Vurpillot, F, Choi, P-P, Li, Y, Raabe, D & Gault, B (2018). On the detection of multiple events in atom probe tomography. Ultramicroscopy 189, 5460.Google Scholar
Rolander, U & Andrén, H-O (1989). Statistical correction for pile-up in the atom-probe detector system. Le Journal de Physique Colloques 50, C8-529C8-534.Google Scholar
Tsong, TT (1990). Atom-probe Field ion Microscopy: Field ion Emission and Surfaces and Interfaces at Atomic Resolution. Cambridge: Cambridge University Press. Available at http://ebooks.cambridge.org/ref/id/CBO9780511599842 (retrieved July 9, 2018).Google Scholar
Vallerga, JV & McPhate, JB (2000). Optimization of the readout electronics for microchannel plate delay line anodes. Fineschi, S, Korendyke, CM, Siegmund, OHW & Woodgate, BE (Eds.), pp. 3442. Available at http://proceedings.spiedigitallibrary.org/proceeding.aspx?articleid=919916 (retrieved July 9, 2018).Google Scholar
Vurpillot, F (2016). Field Ion emission mechanisms. In Atom Probe Tomography, Lefebvre-Ulrikson, W, Vurpillot, F and Sauvage, X (Eds.), pp. 1772. London, United Kingdom: Academic Press. Available at http://linkinghub.elsevier.com/retrieve/pii/B9780128046470000024 (retrieved July 9, 2018).Google Scholar
Yao, L, Gault, B, Cairney, JM & Ringer, SP (2010). On the multiplicity of field evaporation events in atom probe: A new dimension to the analysis of mass spectra. Philos Mag Lett 90, 121129.Google Scholar