Hostname: page-component-78c5997874-j824f Total loading time: 0 Render date: 2024-11-17T16:01:42.723Z Has data issue: false hasContentIssue false

Quicktime as a Storage Medium for Dynamic Data Sets in In-Situ Electron Microscopy

Published online by Cambridge University Press:  02 July 2020

John F. Mansfield*
Affiliation:
North Campus Electron Microbeam Analysis Laboratory 417 SRB, University of Michigan, 2455 Hayward, Ann Arbor, MI, 48109-2143 http://emalwww.engin.umich.edu/people/jfmjfm/
Get access

Extract

The field of in-situ electron microscopy has recently become very active. Microscopy and Microanalysis 1997 was host to an extended symposium devoted entirely to in-situ studies. Also, a recent Winter School sponsored by Arizona State University was devoted entirely to in-situ electron microscopy and drew over 90 attendees. Examination of the presentations and papers in these in-situ symposia has revealed that the researchers involved still have problems acquiring, managing and storing and manipulating their data. An in-situ experiment, by its very nature, is dynamic and recording micrographs is typically not the optimum method of image acquisition. Videotape is the preferred medium. High grade S-video recording of experiments permits the extraction of single frames of reasonable quality from the tapes for presentation and publication. There are, however, a number of problems with video recording. During in-situ studies a number of variables in the sample environment are changing, e.g. the pressure, the temperature, the stress, the strain and the microscope parameters (accelerating voltage, beam current, magnification, specimen tilt, etc.).

Type
Advances in Remote Microscopy, Instrument Automation and Data Storage
Copyright
Copyright © Microscopy Society of America

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

References:

1Gai, P., “Unveiling Novel Reaction Processes in Catalysis by Environmental-HREM (EHREM)”, Microscopy & Microanalysis 3, Supplement 2, (1997) 617.CrossRefGoogle Scholar
2Sinclair, R., Itoh, T., Lee, H.J. and Kwon, K.W., “In-Situ HREM of Reactions at Interfaces”, Microscopy & Microanalysis 3, Supplement 2, (1997) 621.CrossRefGoogle Scholar
3Inkson, B.J. and Ruhle, M., “HREM Analysis of TiB2 - Ti3B4 Precipitates Grown In-Situ in TiAl”, Microscopy & Microanalysis 3, Supplement 2, (1997) 625.CrossRefGoogle Scholar
4 “1998 ASU Winter School on In-Situ Electron Microscopy”, proceedings to be published.Google Scholar
11Mansfield, J.F., Thouless, M., Stefano, J.A. & Holbrook, J, “Design and Construction of a Quantitative Uniaxial Straining Stage for the Environmental SEM”, This proceedings.Google Scholar