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Multi-Scale Correlative Microscopy Investigation of Both Structure and Chemistry of Deformation Twin Bundles in Fe–Mn–C Steel

Published online by Cambridge University Press:  08 October 2013

Ross K.W. Marceau ,
Ivan Gutierrez-Urrutia ,
Michael Herbig ,
Katie L. Moore ,
Sergio Lozano-Perez  and
Dierk Raabe
Ross K.W. Marceau*
Affiliation:
Max-Planck-Institut für Eisenforschung, Max-Planck-Straße 1, 40237 Düsseldorf, Germany
Ivan Gutierrez-Urrutia
Affiliation:
Max-Planck-Institut für Eisenforschung, Max-Planck-Straße 1, 40237 Düsseldorf, Germany
Michael Herbig
Affiliation:
Max-Planck-Institut für Eisenforschung, Max-Planck-Straße 1, 40237 Düsseldorf, Germany
Katie L. Moore
Affiliation:
Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH, UK
Sergio Lozano-Perez
Affiliation:
Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH, UK
Dierk Raabe
Affiliation:
Max-Planck-Institut für Eisenforschung, Max-Planck-Straße 1, 40237 Düsseldorf, Germany
*
*Corresponding author.[email protected]
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Abstract

A multi-scale investigation of twin bundles in Fe–22Mn–0.6C (wt%) twinning-induced plasticity steel after tensile deformation has been carried out by truly correlative means; using electron channelling contrast imaging combined with electron backscatter diffraction, high-resolution secondary ion mass spectrometry, scanning transmission electron microscopy, and atom probe tomography on the exact same region of interest in the sample. It was revealed that there was no significant segregation of Mn or C to the twin boundary interfaces.

Keywords

correlative microscopyelectron channelling contrast imaginghigh-resolution secondary ion mass spectrometryscanning transmission electron microscopyatom probe tomographyaustenitic steelstwinning
Type
Materials Applications
Information
Microscopy and Microanalysis , Volume 19 , Issue 6 , December 2013 , pp. 1581 - 1585
Copyright
Copyright © Microscopy Society of America 2013 

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