The authors acknowledge funding from BP through the BP International Centre for Advanced Materials (BP-ICAM) and the Engineering and Physical Sciences Research Council (EPSRC) (EP/L01680X) through the Materials for Demanding Environments Centre for Doctoral Training. This work was also supported by the Henry Royce Institute for Advanced Materials (EP/R00661X/1, EP/S019367/1, EP/P025021/1 and EP/P025498/1) and the MIDAS Zr grant EP/S01702X/1. We would like to thank Jacobs for supplying the autoclave facilities and financial support.
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