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Extending lab-based X-ray nanotomography of low Z and porous materials to larger sample volumes without compromising resolution

Published online by Cambridge University Press:  30 July 2021

Silvan Englisch ,
Janis Wirth ,
Dominik Drobek ,
Benjamin Apeleo Zubiri  and
Erdmann Spiecker
Silvan Englisch
Affiliation:
Institute of Micro- and Nanostructure Research (IMN) & Center for Nanoanalysis and Electron Microscopy (CENEM), Interdisciplinary Center for Nanostructured Films (IZNF), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Erlangen, Germany, Erlangen, Bayern, Germany
Janis Wirth
Affiliation:
Institute of Micro- and Nanostructure Research (IMN) & Center for Nanoanalysis and Electron Microscopy (CENEM), Interdisciplinary Center for Nanostructured Films (IZNF), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Erlangen, Germany, Erlangen, Bayern, Germany
Dominik Drobek
Affiliation:
Institute of Micro- and Nanostructure Research (IMN) & Center for Nanoanalysis and Electron Microscopy (CENEM), Interdisciplinary Center for Nanostructured Films (IZNF), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Erlangen, Germany, Erlangen, Bayern, Germany
Benjamin Apeleo Zubiri
Affiliation:
Institute of Micro- and Nanostructure Research (IMN) & Center for Nanoanalysis and Electron Microscopy (CENEM), Interdisciplinary Center for Nanostructured Films (IZNF), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Erlangen, Germany, Erlangen, Bayern, Germany
Erdmann Spiecker
Affiliation:
Institute of Micro- and Nanostructure Research (IMN) & Center for Nanoanalysis and Electron Microscopy (CENEM), Interdisciplinary Center for Nanostructured Films (IZNF), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg (FAU), Erlangen, Germany, Erlangen, Bayern, Germany

Abstract

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Type
Nanoscale x-ray and Electron Microscopy Techniques and Applications in Material Science
Information
Microscopy and Microanalysis , Volume 27 , Supplement S1 , August 2021 , pp. 1218 - 1221
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Copyright
Copyright © The Author(s), 2021. Published by Cambridge University Press on behalf of the Microscopy Society of America

References

Apeleo, B., et al. , (2020) "Correlative Laboratory Nano-CT and 360° Electron Tomography of Macropore Structures in Hierarchical Zeolites." Adv. Mater. Interfaces, 2001154.Google Scholar
Du, M., et al. , (2018). "X-ray tomography of extended objects: a comparison of data acquisition approaches." Journal of the Optical Society of America a-Optics Image Science and Vision. 35(11): p. 1871-1879.Google ScholarPubMed
Wang, J., et al. (2012). "Automated markerless full field hard x-ray microscopic tomography at sub-50 nm 3-dimension spatial resolution." Applied Physics Letters 100(14): 143107.CrossRefGoogle Scholar
van Aarle, W., et al. (2016). "Fast and flexible X-ray tomography using the ASTRA toolbox." Optics Express, 24(22): p. 25129-25147.CrossRefGoogle ScholarPubMed
Wirth, J., et al. ,(2019). "Structural Analysis of Liquid Metal Catalysts in Porous Silica Utilizing Nano-CT and Analytical Transmission Electron Microscopy." Microscopy and Microanalysis, 25(S2): p. 422-423.CrossRefGoogle Scholar
van Heel, M., et al. (2005). "Fourier shell correlation threshold criteria." Journal of Structural Biology 151(3):50-262.CrossRefGoogle ScholarPubMed
7. We gratefully acknowledge financial support by the German Research Foundation (DFG) within the frameworks of the research training group GRK1896 “In situ Microscopy with Electrons, X-rays and Scanning Probes”, the project SP648/8 “High-resolution X-ray microscopy for correlative tomography, high throughput screening and in situ mechanical testing of structural and functional materials” (Project ID 316992193), the Collaborative Research Centre 1411 “Design of Particulate Products” (Project ID 416229255) and the Collaborative Research Centre 1452 "Catalysis at Liquid Interfaces". We thank P. Wasserscheid, W. Schwieger and their research groups for providing the SCALMS and Zeolite samples used in this study.Google Scholar