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Conditional Random Surveying for Particle Deposition on a Mica Surface

Published online by Cambridge University Press:  28 September 2007

Jianzhong Fu ,
Elia V. Eschenazi  and
Kyriakos D. Papadopoulos
Jianzhong Fu
Affiliation:
Department of Chemical & Biomolecular Engineering, Tulane University, New Orleans, LA 70118, USA Department of Physics and Engineering, Xavier University, New Orleans, LA 70125, USA
Elia V. Eschenazi
Affiliation:
Department of Mathematics, Physics and Computer Science, University of the Sciences in Philadelphia, Philadelphia, PA 19104, USA
Kyriakos D. Papadopoulos
Affiliation:
Department of Chemical & Biomolecular Engineering, Tulane University, New Orleans, LA 70118, USA
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Abstract

In using microscopic imaging techniques, unbiased selection of sampling areas is often critical when judgment has to be used to find regions of interest. A conditional random sampling was designed to survey hematite particles on a mica surface using tapping-mode atomic force microscopy, based on three adapted-systematic-sampling methods designed to exclude subjective bias by limiting the freedom of arbitrarily selecting sampling areas. The results of these surveying methods were compared with the average particle surface density modeled by Poisson distribution. It was found that the conditional random sampling could survey particles effectively and improve the data reliability significantly. Ten population-known images from the same mica sheet were used to evaluate these methods, and an average relative error of 12% (maximum 21%) was obtained using the conditional random method with six sampling areas. It was used to investigate the effects of common organic pollutants, benzene, toluene, ethylbenzene, and xylenes on the transport of soil colloids.

Keywords

AFMBTEXhematitemicaparticle numberrandom sampling
Type
MATERIALS APPLICATIONS
Information
Microscopy and Microanalysis , Volume 13 , Issue 5 , October 2007 , pp. 358 - 364
Copyright
© 2007 Microscopy Society of America

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References

REFERENCES

Andriani, G.F. & Walsh, N. (2002). Physical properties and textural parameters of calcarenitic rocks: Qualitative and quantitative evaluations. Eng Geol 67, 5–15.Google Scholar
Ferris, M.M., McCabe, M.O., Doan, L.G. & Rowlen, K.L. (2002). Rapid enumeration of respiratory viruses. Anal Chem 74, 1849–1856.Google Scholar
Foreman, E.K. (1991). Survey Sampling Principles. New York: Marcel Dekker, Inc.
Francis, H.W., Rivas, A., Lehar, M., Saito, Y., Mouton, Peter R. & Ryugo, David K. (2006). Efficient quantification of afferent cochlear ultrastructure using design-based stereology. J Neurosci Methods 150, 150–158.Google Scholar
Geuna, S. (2005). The revolution of counting “tops”: Two decades of the disector principle in morphological research. Microsc Res Techn 66, 270–274.Google Scholar
Gillis, R.J. & Iglewski, B.H. (2004). Azithromycin retards Pseudomonas aeruginosa biofilm formation. J Clin Microbiol 42, 5842–5845.Google Scholar
Gundersen, H.J., Bendtsen, T.F., Korbo, L., Marcussen, N., Moller, A., Nielsen, K., Nyengaard, J.R., Pakkenberg, B., Sorensen, F.B., Vesterby, A. & West, M.J. (1988). Some new, simple and efficient stereological methods and their use in pathological research and diagnosis. Apmis 96, 379–394.Google Scholar
Herrera, A.M., Martinez, E.C. & Seow, C.Y. (2004). Electron microscopic study of actin polymerization in airway smooth muscle. Am J Physiol Lung Cell Mol Physiol 286, L1161–L1168.Google Scholar
King, M.A., Scotty, N., Klein, R.L. & Meyer, E.M. (2002). Particle detection, number estimation, and feature measurement in gene transfer studies: Optical fractionator stereology integrated with digital image processing and analysis. Methods 28, 293–299.Google Scholar
Lavalle, P., Gergely, C., Lustig, A. & Ball, V. (2000). Critical analysis of the apoferritin adsorption at solid–liquid interfaces in the framework of a particular adsorption model. J Chem Phys 113, 8212–8224.Google Scholar
Liu, Z.H. & Brown, N.M.D. (1997). The influence of imaging conditions on the appearance of lattice-resolved AFM images of mica surfaces. J Phys D Appl Phys 30, 2503–2508.Google Scholar
Lynnerup, N., Frohlich, B. & Thomsen, JL. (2006). Assessment of age at death by microscopy: Unbiased quantification of secondary osteons in femoral cross sections. Forensic Sci Int 159(Suppl. 1), S100–S103.Google Scholar
Miyamoto, K. & Hoshimiya, T. (2006). Measurement of the amount and number of pollen particles of Cryptomeria japonica (Taxodiaceae) by imaging with a photoacoustic microscope. IEEE Trans Ultrason Ferroelectric Freq Contr 53, 586–591.Google Scholar
Mouton, P.R. (2002). Principles and Practices of Unbiased Stereology: An Introduction for Bioscientists. Baltimore, MD: Johns Hopkins University Press.
Puntes, V.F., Gorostiza, P., Aruguete, D.M., Bastus, N.G. & Alivisatos, A.P. (2004). Collective behaviour in two-dimensional cobalt nanoparticle assemblies observed by magnetic force microscopy. Nat Mater 3, 263–268.Google Scholar
Rose, D., Durose, K., Palosz, W., Szczerbakow, A. & Grasza, K. (1998). Methods of dislocation distribution analysis and inclusion identification with application to CdTe and (Cd, Zn)Te. J Phys D Appl Phys 31, 1009–1016.Google Scholar
Semmler, M., Mann, E.K., Ricka, J. & Borkovec, M. (1998). Diffusional deposition of charged latex particles on water–solid interfaces at low ionic strength. Langmuir 14, 5127–5132.Google Scholar
Sriram, S., Balasubramaniam, R., Mungole, M.N. & Baligidad, R.G. (2005). Effect of cerium addition on microstructures of carbon-alloyed iron aluminides. Bull Mater Sci 28, 547–554.Google Scholar
Sterio, D.C. (1984). The unbiased estimation of number and sizes of arbitrary particles using the disector. J Microsc 134, 127–136.Google Scholar
Wen, L., Wu, R.C., Eschenazi, E. & Papadopoulos, K. (2002). AFM of amidine latex particles attachment on mica. Colloid Surf Physicochem Eng Aspect 197, 157–165.Google Scholar
Yamamoto, S., Yoshino, I., Shimazaki, T., Murohashi, M., Hevner, R.F., Lax, I., Okano, H., Shibuya, M., Schlessinger, J. & Gotoh, N. (2005). Essential role of Shp2-binding sites on FRS2{alpha} for corticogenesis and for FGF2-dependent proliferation of neural progenitor cells. Proc Natl Acad Sci USA 102, 15983–15988.Google Scholar