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Transmission Electron Microscopy Characterization of Thermomechanically Treated Al3Ti–(8, 10, 15)% Cr Intermetallics

Published online by Cambridge University Press:  06 August 2013

Ok Jun Jang
Affiliation:
School of Advanced Materials Science & Engineering, Sungkyunkwan University, Suwon 440-746, SouthKorea
Cheol-Woong Yang
Affiliation:
School of Advanced Materials Science & Engineering, Sungkyunkwan University, Suwon 440-746, SouthKorea
Dong Bok Lee*
Affiliation:
School of Advanced Materials Science & Engineering, Sungkyunkwan University, Suwon 440-746, SouthKorea
*
*Corresponding author. E-mail: [email protected]
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Abstract

The ordered L12-type Al3Ti–(8, 10, 15)% Cr intermetallic compounds, namely, Al67Ti25Cr8, Al66Ti24Cr10, and Al59Ti26Cr15, were prepared by induction melting followed by thermomechanical treatment. Their microstructure, compositional variation, and crystal structure were characterized using X-ray diffraction, optical microscopy, and scanning and transmission electron microscopy equipped with energy-dispersive spectroscopy. The Al67Ti25Cr8 alloy consisted of the L12-Al3Ti matrix and precipitates of α2-Ti3Al, D022-Al3Ti, and γ-TiAl. The Al66Ti24Cr10 and Al59Ti26Cr15 alloys consisted of the L12-Al3Ti matrix and grains of α-TiAl and β-Cr.

Type
Research Article
Copyright
Copyright © Microscopy Society of America 2013 

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References

Jewett, T.J., Ahrens, B. & Dahms, M. (1996). Phase equilibria involving the τ-L12 and TiAl2 phases in the Ti–Al–Cr system. Intermetallics 4, 543556.10.1016/0966-9795(96)00044-1Google Scholar
Kim, G.H. & Ahn, J.P. (2006). Phase identification of nano-phase materials using convergent beam electron diffraction (CBED) technique. Korean J Microsc 1, 4756.Google Scholar
Kim, G.H., Kim, H.S. & Kum, D.W. (1996). Simple procedure for phase identification using convergent beam electron diffraction patterns. Microsc Res Techniq 33, 510515.10.1002/(SICI)1097-0029(19960415)33:6<510::AID-JEMT6>3.0.CO;2-O3.0.CO;2-O>Google Scholar
Klansky, J.L., Nic, J.P. & Mikkola, D.E. (1994). Structure/property observations for Al–Ti–Cr intermetallic alloys. J Mater Res 9, 255258.10.1557/JMR.1994.0255Google Scholar
Kumar, K.S. & Brown, S.A. (1996). Response to three-point bending of the forged L12 compound Al66Ti25Cr9. Intermetallics 4, 231244.10.1016/0966-9795(95)00042-9Google Scholar
Lee, J.K., Oh, M.W., Oh, M.H. & Wee, D.M. (2003). Phase stability of L12 based alloys in Al–Ti–Cr systems. Intermetallics 11, 857865.10.1016/S0966-9795(03)00084-0Google Scholar
Mabuchi, H., Tsuda, H., Matsui, T. & Morii, K. (1997). Microstructure and mechanical properties of ternary L12 intermetallic compound in Al–Ti–Cr system. Mater Trans JIM 38, 560565.10.2320/matertrans1989.38.560Google Scholar
Nakayama, Y. & Mabuchi, H. (1993). Formation of ternary L12 compounds in Al3Ti-base alloys. Intermetallics 1, 4148.10.1016/0966-9795(93)90020-VGoogle Scholar
Nic, J.P., Klansky, J.L. & Mikkola, D.E. (1992). Structure/property observations for Al–Ti–Cr alloys near the cubic (Al,Cr)3Ti phase. Mater Sci Eng A152, 132137.10.1016/0921-5093(92)90058-9Google Scholar
Parfitt, L.J., Smialek, J.L., Nic, J.P. & Mikkola, D.E. (1991). Oxidation behavior of cubic phases formed by alloying aluminum-titanium (Al3Ti) with chromium and manganese. Scripta Metall Mater 25, 727731.10.1016/0956-716X(91)90123-IGoogle Scholar
Raghava, V. (2005). Al–Cr–Ti. J Phase Equilib Diff 26, 349356.Google Scholar
Stein, F., Zhang, L.C., Sauthoff, G. & Palm, M. (2001). TEM and DTA study on the stability of Al5Ti3- and h-Al2Ti-superstructures in aluminium-rich TiAl alloys. Acta Mater 49, 29192932.10.1016/S1359-6454(01)00208-7Google Scholar
Xu, H., Jin, Z. & Wang, R. (1997). Study on the phase equilibria of the Al–Cr–Ti system at 1050°C. Scripta Mater 37, 14691473.10.1016/S1359-6462(97)00298-4Google Scholar