Hostname: page-component-586b7cd67f-t7czq Total loading time: 0 Render date: 2024-11-26T11:46:54.318Z Has data issue: false hasContentIssue false

Fractographic Evaluation of Thermally Stressed Single Crystal Sapphire

Published online by Cambridge University Press:  02 July 2020

S.D. Wajer
Affiliation:
Technical Services Department, Johns Hopkins University, Applied Physics Laboratory, Laurel, Maryland, 20723
P.H. Cohen
Affiliation:
Technical Services Department, Johns Hopkins University, Applied Physics Laboratory, Laurel, Maryland, 20723
Get access

Extract

Optical, video and scanning electron microscopic observations show fractographic features that are used to determine the crack propagation direction and crack origin in thermally stressed single crystal sapphire hemispherical shells. These features have been typically identified in materials with symmetrically applied stresses and simple geometries. This fractographic evaluation of sapphire is unusual because of the hemispherical geometry and complex mechanical and thermal stress conditions. Computer models predict the thermal stress response of the sapphire from fast acting asymmetrical heating patterns generated during controlled laboratory testing. These experimental tests are conducted to validate the computer model predictions. When an experimental structure fails to meet the survival limits predicted by the computer model, a fractographic evaluation is conducted to determine fracture mode and to locate the crack initiation site.

Fractured pieces are examined and photographed using a low magnification, binocular optical microscope and a high resolution video camera with digitizing capabilities.

Type
Microscopy and Microanalysis in the “Real World”
Copyright
Copyright © Microscopy Society of America

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

References:

1.Michalske, T. A., in Engineered Materials Handbook, (ASM Int'l, 1991) 4:652.Google Scholar
2.Richerson, D. W., Metals Handbook, (1986) 11:744.Google Scholar
3.Rice, R. W., in Fractography of Ceramics and Glass, (ASTM,1984)5.CrossRefGoogle Scholar
4.Preston, F. W., J. Am. Ceram. Soc, Vol 18, (1935)175.CrossRefGoogle Scholar
5.Varner, J. R., in Engineered Materials Handbook, (ASM Int'l, 1991) 4:635.Google Scholar
6.Frazer, R. K. and Lutz, S. A. are gratefully acknowledged for technical support and for providing the sapphire shells used in this study.Google Scholar