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Pressure-induced nanocrystallization of Zr55Al10Ni5Cu30 bulk metallic glass

Published online by Cambridge University Press:  31 January 2011

Jia Zhang ,
K. Q. Qiu ,
A. M. Wang ,
H. F. Zhang ,
M. X. Quan  and
Z. Q. Hu
Jia Zhang*
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People's Republic of China
K. Q. Qiu
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People's Republic of China
A. M. Wang
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People's Republic of China
H. F. Zhang
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People's Republic of China
M. X. Quan
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People's Republic of China
Z. Q. Hu
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People's Republic of China
*
a) Address all correspondence to this author. e-mail: [email protected]
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Abstract

The effect of pressure on the crystallization behavior of Zr55Al10Ni5Cu30 bulk metallic glass was investigated by differential scanning calorimetry, x-ray diffraction, and transmission electron microscopy. Although the crystallization products under high pressure were about the same as those under ambient pressure, the evident changes in the relative crystallization fraction of each phase were observed. The applied pressure enhanced the crystallization temperature. Pressure annealing of the bulk metallic glass produced a composite with dispersion of very fine nanocrystallites in the amorphous matrix. A full nanocrystallization was obtained for the sample annealed under 5 GPa at 793 K. The mechanism for the pressure-induced nanocrystallization is discussed.

Type
Articles
Information
Journal of Materials Research , Volume 17 , Issue 11 , November 2002 , pp. 2935 - 2939
Copyright
Copyright © Materials Research Society 2002

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